## Syllabus 2022-23 - 14212010 - Chemical Engineering (Ingeniería química)

Caption
• Level 1: Tutorial support sessions, materials and exams in this language
• Level 2: Tutorial support sessions, materials, exams and seminars in this language
• Level 3: Tutorial support sessions, materials, exams, seminars and regular lectures in this language
 DEGREE: Grado en Ingeniería de recursos energéticos FACULTY: SCHOOL OF ENGINEERING OF LINARES ACADEMIC YEAR: 2022-23 COURSE: Chemical Engineering
SYLLABUS
1. COURSE BASIC INFORMATION
 NAME: Chemical Engineering CODE: 14212010 ACADEMIC YEAR: 2022-23 LANGUAGE: English LEVEL: 1 ECTS CREDITS: 9.0 YEAR: 3 SEMESTER: SC
2. LECTURER BASIC INFORMATION
 NAME: MATEO QUERO, MARÍA DE LA SOLEDAD DEPARTMENT: U122 - INGENIERÍA QUIM.,AMBIENTAL Y DE LOS MAT. FIELD OF STUDY: 555 - INGENIERÍA QUÍMICA OFFICE NO.: D - 018 E-MAIL: smateo@ujaen.es P: 648642 WEBSITE: - ORCID: https://orcid.org/0000-0002-0359-3265 LANGUAGE: - LEVEL: 1
3. CONTENT DESCRIPTION

BLOCK I. INTRODUCTION TO CHEMICAL ENGINEERING.

TOPIC 1. INTRODUCTION TO CHEMICAL ENGINEERING.

Concept of Chemical Engineering. Basic or Unit Operations: concept. Continuous, discontinuous and semi-continuous operations. Ways of carrying out basic operations by transfer of matter: continuous and discontinuous contact; parallel, countercurrent and cross flow. Classification of basic operations.

BLOCK II. MACROSCOPIC BALANCES OF MATTER.

TOPIC 2. MACROSCOPIC BALANCES OF MATTER.

Introduction. General equation of the macroscopic balance of matter. Concept of calculation basis. Balances of matter in steady state without chemical reaction. Steady state balances of matter with chemical reaction. Introduction to the balances of matter in non-steady state. Examples and model problems (the English version is also considered).

BLOCK III: ENERGY BALANCES.

TOPIC 3. MACROSCOPIC ENERGY BALANCES.

General equation of the macroscopic energy balance. Enthalpy balance in steady state without chemical reaction. Enthalpy balance in stationary regime with chemical reaction. Examples and model problems (the English version is also considered).

BLOCK IV: INTRODUCTION TO TRANSPORT PHENOMENA .

TOPIC 4. INTRODUCTION TO THE STUDY OF TRANSPORT PHENOMENA.

Introduction to the theoretical models of transport phenomena. Mechanisms of molecular and turbulent transport. Kinetic equations in molecular transport: Newton's, Fourier's and Fick's laws. Turbulent transport: individual and global transport coefficients.

BLOCK V: INTRODUCTION TO HEAT TRANSFER.

TOPIC 5. INTRODUCTION TO HEAT TRANSFER.

Heat transfer mechanisms. General equation of heat transport in solids by conduction: thermal conductivity. Introduction to heat convection: natural or free and forced convection. Expressions for the calculation of the heat transfer coefficient by convection. Mechanism of heat transfer by radiation: black and gray objects. Stefan-Boltzmann's law equation.

BLOCK VI/BLOCK VII: INTRODUCTION TO MATTER TRANSFER/MATTER TRANSFER OPERATIONS.

TOPIC 6: LIQUID (L)-STEAM (S) EQUILIBRIUM.

Equilibrium between phases. L-S equilibrium. Equilibrium diagram. Laws of L-S equilibrium for ideal systems. Concept of absolute and relative volatility. Influence of volatility on equilibrium. Influence of temperature on vapor pressure. Problems (the English version is also considered).

TOPIC 7: DISTILLATION.

Concept of distillation. Distillation methods. Simple distillations: sudden or equilibrium distillation and differential or open distillation. Problems.

TOPIC 8: CONTINUOUS RECTIFICATION OF BINARY MIXTURES.

Concept. Columns of plates. Calculation of the number of theoretical plates necessary to achieve a given separation and position of the feed plate: McCabe-Thiele graphical method. Minimum reflux ratio. Total reflux: minimum number of plates. Optimal reflux ratio. Problems.

TOPIC 9: LIQUID-LIQUID EXTRACTION.

Introduction to liquid-liquid equilibrium. Immiscible and miscible phases. Equilibrium diagrams. Single, repeated and countercurrent contact. Basic concepts: binodal curve and partition lines. Exercises.

BLOCK VIII: MATTER AND HEAT TRANSFER OPERATIONS.

TOPIC 10: EVAPORATION.

Generalities. Vapor balance. Types of evaporators. Evaporation capacity. Economy of an evaporator. Single effect evaporation: Calculation. Multiple effect evaporator: Calculation. Problems.

BLOCK IX: LABORATORY PRACTICES.

Balance of matter in non-steady state.
Energy balance.
Refractometry.
Natural convection.
Vapor-liquid equilibrium.
Differential distillation.
Vapor entrainment distillation.

BLOCK X: SEMINARS.

SEMINAR I: PHYSICAL QUANTITIES AND SYSTEMS OF UNITS .

Physical quantities and their measurement. Fundamental and derived quantities. Systems of units. International system of units: advantages and limitations. Direct and indirect methods of measurement. Scientific notation and prefixes. Transformation of units from one system to another. Accuracy of instruments in measurements of different magnitudes and types of errors.

SEMINAR II: FUNDAMENTALS AND PRELIMINARY ASPECTS RELATED TO BLOCK 1 OF LABORATORY PRACTICES.

SEMINAR III: FUNDAMENTALS AND PRELIMINARY ASPECTS RELATED TO BLOCK 2 OF LABORATORY PRACTICES.

T he contents of this course are intended to contribute to the following Sustainable Development Goals (SDGs):

SDG 12.8: Education for sustainable development

SDG 13.3: Improving education and environmental awareness

4. COURSE DESCRIPTION AND TEACHING METHODOLOGY

In the development of the teaching-learning process, different teaching methodologies will be used depending on the part of the course to be addressed.

1. To develop the theoretical part of the subject methodologies of "expository classes in large group" will be used. Specifically, M1 (lectures) and M2 (conferences). The delivery of a lecture related to the program of the subject, given by a professional of the company, will be adaptive and will take into account the specific circumstances that arise in the academic year in which the teaching is given.

2. In relation to the development of the three practical credits of this subject, methodologies in line with "Classes in groups of practices" will be used. Specifically: exercises proposed by the teacher related to the theoretical program of the subject (M11) will be solved; furthermore, practices will be carried out in the laboratory where the theoretical knowledge acquired will be applied by the students, solving at the same time different problematic situations that may occur in the laboratory; all this actions imply that teaching methodologies such as M11, M6 and M9 will be developed. Also closely related to the practical activities are the development of seminars given on specific aspects of the program, or with the practices to be carried out in the laboratory (M7). Finally, students may be proposed to carry out certain works related to the contents of the program, which must be presented and exposed to the rest of their classmates so involving, after the exhibition, a discussion by the attendees in relation to the work presented (M12 and M8).

Students with special educational needs should contact the Student Attention Service (Servicio de Atención y Ayudas al Estudiante) in order to receive the appropriate academic support

5. ASSESSMENT METHODOLOGY

Students may choose between two evaluation systems in this course:

- Continuous evaluation and

- Single evaluation

In the case of selecting the continuous evaluation system, the chosen criteria and the weight assigned to each activity are those one specified above. Class attendance will be valued with 10% of the final mark, by means of a daily control of attendance and an active and participative attitude in class. The theoretical exam will involve the resolution of problems and theoretical questions related to the course program, having been dealt with during the course (50%); in this way the students will have to demonstrate the acquisition of the competences CBB3, CC3, CER4, CG4, CC12, CG5 and CG6. The students will have to hand in questions and problems, previously established and/or assigned, as well as a practice notebook; the evaluation of these last aspects will represent 40% of the final grade of the course (specifically, the grade of the practice notebook will represent 20% of the total mark); the completion of works, cases or exercises will be associated with the procurement of the competences: CBB3, CC3, CER4, CG4, CG4, CC12, CG5 and CG6. This system will allow the evaluation of the learning result: Result-07.

In order to pass the subject, the score obtained in the theoretical exam must be at least 4.5. If this value is not exceeded, the score obtained in the evaluation corresponding to the practical activities of the subject will not count in the final mark, so the final rating for the subject will coincide, in this case, with the mark obtained in the theoretical exam. In order to definitively pass the course, the student must obtain a final overall score equal to or higher than 5.0 points.

In the case of selecting the single evaluation system, the final mark will be obtained by means of an exam that covers all the contents of the subject, carried out within the calendar foreseen for the final exams, which will allow to verify that the students have acquired the competences CBB3, CC3, CER4, CG4, CC12, CG5 and CG6, allowing to evaluate the learning result 7.

This evaluation system will be applied both in the ordinary and extraordinary call.

In any case, the evaluation system will be submitted to the provisions of the Regulations of Academic Regime and Student Evaluation of the University of Jaén.

6. BOOKLIST
MAIN BOOKLIST:
• Distillation: principles and practices. Edition: -. Author: Stichlmair, Johann G.. Publisher: Wiley-VCH  (Library)
• Separation process principles. Edition: -. Author: Seader, J. D.. Publisher: John Wiley  (Library)
7. VIRTUAL / CLASSROOM TEACHING SCENARIO

SCENARIO : Groups of students below the limited capacity in the classroom.

The teaching methodology to be used in the development of the teaching-learning process for this subject as well as the different activities to be developed in the theoretical-practical sessions are:

 Training activities developed Format Teaching methodology used 7 practice sessions in teaching laboratories 100% face-to-face, as far as the socio-sanitary situation allows it. Development of 7 practical sessions, each lasting two hours, in the teaching laboratories of the department. 60 theory sessions on the contents of the program 100% face-to-face, as far as the socio-sanitary situation allows it. 60 sessions of participative lectures, each lasting one hour, held in the classroom. 8 sessions of problem solving/exercises. 100% face-to-face, as far as the socio-sanitary situation allows it. Consist of 8 classroom sessions, each lasting one hour. Impartation of Seminars I, II and III 100% face-to-face, as far as the socio-sanitary situation allows it. They will consist of 6 face-to-face classroom sessions, each lasting one hour. 2 sessions for the presentation of group work and performance of an activity related to the presentation. Face-to-face 100% as far as the socio-sanitary situation allows it. They will consist of 2 classroom sessions of one hour each one. Tutorials Face-to-face + on-line Some tutoring sessions will be face-to-face and others on-line (synchronous and asynchronous).

The expository classes in groups (master classes, introductory activities, and conferences, when the situation allows it) will be dedicated to explain contents of fundamentally theoretical character, related to the established topics. Some of these sessions will have as purpose to comment relevant contents previous to the realization of the laboratory practices. They will allow the student to achieve the competences CBB3, CC12, CC3, CER4, CG4, CG5 and CG6.

On the other hand, the practical activities (problem solving, practical exercises, seminars, discussions, exhibitions and laboratory practices), will allow the student to achieve the competences CBB3, CC12, CC3, CER4, CG4, CG5 and CG6.

The theoretical classes will be generally supported by the use of different didactic and audiovisual resources such as: cannon, blackboard, computer, internet, etc. In the laboratory sessions, specific teaching equipment will be used according to the different programmed practices. In addition, the didactic resources available in the UJA library, both in paper and electronic format, as well as other resources available on the Internet, will be used as support teaching materials.

In the case of on-line tutoring, this work will be carried out using tools such as e-mail, teaching platform (PLATEA), google meet, etc.

The evaluation criteria will be the same as those established in the first scenario, corresponding to face-to-face teaching, both for the ordinary and extraordinary call. This system will allow the evaluation of the learning outcome: Result-07.

________________________________________________________________________________________

In the multimodal and/or non face-to-face scenario, when appropriate, the teaching staff involved in teaching reserves the right not to give consent for the capture, publication, retransmission or reproduction of their speech, image, voice and explanations, in the exercise of their teaching functions, within the scope of the University of Jaén.

8. VIRTUAL TEACHING SCENARIO

In this case, the teaching methodology to be used in the development of the teaching-learning process for this subject as well as the different activities to be developed in the theoretical-practical sessions are as follows:

 Training activities developed Format (on-line) Teaching methodology used 7 practical sessions (in replacement of the practical sessions in teaching laboratories) Non-attendance (synchronous and asynchronous modality) Substitution of laboratory practical sessions (2 hours each one) by on-line training activities: - Comments on the practice scripts - Viewing of videos related to contents of interest Calculations with data provided by the teacher 60 theory sessions on the contents of the program Non-attendance (synchronous) 60 sessions of participatory master classes, each one lasting one hour, conducted via videoconference 8 sessions of problem solving/exercises Non-attendance (synchronous) They will consist of 8 synchronous on-line sessions, each lasting one hour, in which practical numerical exercises related to the subject will be solved. Teaching of Seminars I, II and III Non-attendance (synchronous) They will consist of 6 video-conference sessions, each one lasting one hour. 2 sessions for the presentation of group work and performance of an activity related to the presentation. Non-attendance (synchronous) They will consist of 2 non face-to-face sessions that will be carried out by videoconference, of one hour of duration each one, in which expositions and on-line defenses of the proposed work will be contemplated. The following tools characteristic of virtual teaching will be used Mentoring Classroom + Online Some tutoring sessions will be face-to-face and others online (synchronous and asynchronous).

The expository classes in groups (lectures, introductory activities, and conferences, when the situation allows it) will be dedicated to explain contents of fundamentally theoretical character, related to the principles and basic operations object of study of chemical engineering. They will allow the student to achieve the competences CBB3, CC12, CC3, CER4, CG4, CG5 and CG6.

On the other hand, the practical activities (problem solving, practical exercises, seminars, expositions and debates), will allow the student to reach the competences CBB3, CC12, CC3; CER4, CG4, CG5 and CG6.

The synchronous non face-to-face teaching will be given by videoconference using the Hangouts meet tool (from Google) or any other videotelephony tool. Some ICT resources will be used, together with the virtual teaching platform as well as the use of e-mail as mechanisms that will allow the teaching-learning process to be carried out. These same tools will be used to carry out the tutoring work.

The evaluation criteria and instruments will be the following:

 Aspect Criteria Instrument/Format Peso Attendance and/or participation in face-to-face and/or virtual activities Active participation in programmed activities. Participation in the debates Observation and teacher's notes (attendance lists). On-line synchronous 10% Theoretical concepts of the subject Mastery of the theoretical and operative knowledge of the subject matter Theoretical exam on-line synchronous 40% Completion of work, cases or exercises Delivery of well solved problems. Attendance to practices is mandatory. Delivery of the practice notebook. Defense of a problem and/or work related to the syllabus of the subject. Evaluation of the structure, quality of the documentation and presentation of the work (related to Topic 5 of the theoretical program of the course) Delivery and/or defense of a practical exercise/problems (on-line synchronous and asynchronous). o Delivery of a laboratory practice report (asynchronous). o Delivery and defense of an assigned work (evaluation by rubric). On-line synchronous 50%  20% delivery of exercises - 20% internship report - 10% delivery and presentation of the proposed work

In order to pass the subject, students must pass an on-line theoretical-practical exam that will represent 40% of the total weight of the evaluation. The evaluation of the practical part of the course will be done through the delivery of a practical report in relation to the teaching activities developed that will represent 40% of the final grade (20% the delivery of the proposed exercises and 20% the report of the activities that replace the laboratory practices), as well as the realization of a group work (or individual, if considered more convenient) related to the subject of the course (example: Topic 5); the student will have to defend this work before the teacher and carry out the activity/activities suggested and its weight in the final evaluation will be 10%. Finally, attendance will be controlled, valuing the participation and active attitude in class, which will represent 10% of the final mark. To pass the subject, the student must obtain a final overall grade equal to or higher than 5.0 points.

Note 1: In order to pass the course, in general, the score obtained in the theoretical exam must be at least 4.0. If this value is not exceeded, the score obtained in the evaluation corresponding to the practical activities of the course will not count in the final grade of the same, so that it will coincide, in this case, with the grade obtained in the theoretical exam.

Note 2 : The above evaluation system will be applied to those students who can regularly attend the virtual sessions (continuous evaluation system). However, there are specific cases of students who cannot follow the above mentioned system. In that case, the student would be evaluated exclusively by means of the written exam, carried out within the calendar foreseen for the final exams, and would pass the subject by obtaining a minimum grade equal to 5.0 points.

This evaluation system will be applicable for both the ordinary and extraordinary exams.

This system will allow the evaluation of the learning result Result-07.

________________________________________________________________________________________

In the multimodal and/or non face-to-face scenario, when appropriate, the teaching staff involved in the teaching reserves the right not to give consent for the capture, publication, retransmission or reproduction of their speech, image, voice and explanations of professorship, in the exercise of their teaching functions, within the scope of the University of Jaén.

DATA PROTECTION CLAUSE (on line exams)

Institution in charge of data processing: Universidad de Jaén, Campus Las Lagunillas, s/n, 23071 Jaén

Data Protection Delegate: dpo@ujaen.es

Purpose: In accordance with the Universities Law and other national and regional regulations in force, carrying out exams and assessment tests corresponding to the courses students are registered in. In order to avoid frauds while sitting the exam, the exam will be answered using a videoconference system, being able the academic staff of the University of Jaén to compare and contrast the image of the person who is answering the exam with the student's photographic files. Likewise, in order to provide the exam with evidential content for revisions or claims, in accordance with current regulation frameworks, the exam will be recorded and stored.

Legitimacy: compliance with legal obligations (Universities Law) and other national and regional regulations currently in force.

Addressees: service providers who are the owners of the platforms where the exams are carried out and with whom the University of Jaén has signed the corresponding data access contracts.

Storage periods: those established in current in force regulations. In the specific case of exam videoconference recordings, not before the examination records and transcripts are closed or the exam can still be reviewed or challenged.

Rights: you can exercise your right of access, amendment, cancellation, opposition, suppression, limitation and portability by sending a letter to the postal or electronic address indicated above. In the event that you consider that your rights have been violated, you may submit a complaint to the Andalusian Council for Transparency and Data Protection www.ctpdandalucia.es

CLASS RECORDING CLAUSE PERSONAL DATA PROTECTION

Person in charge: Universidad de Jaén, Paraje Las Lagunillas, s/n; Tel.953 212121; www.ujaen.es

Data protection delegate (DPO): TELEFÓNICA, S.A.U. ; Email: dpo@ujaen.es

Procedure aim: To manage proper recordings of teaching sessions with the aim of facilitating learning process under a multimodal and/or online teaching

Period for record storage: Images will be kept during legal term according to regulations in force

Legitimacy: Data will be managed according to legal regulations (Organic Law 6/2001, December 21, on Universities) and given consent provided by selecting corresponding box in legal admission documents

Data recipients (transfers or assignments): Any person allowed to get access to every teaching modality

Rights: You may exercise your rights of access, rectification, cancellation, portability, limitation of processing, deletion or, where appropriate, opposition. To exercise these rights, you must submit a written request to the Information, Registration and Electronic Administration Service of the University of Jaen at the address above, or by e-mail to the address above. You must specify which of these rights you are requesting to be satisfied and, at the same time, you must attach a photocopy of your ID card or equivalent identification document. In case you act through a representative, legal or voluntary, you must also provide a document that proves this representation and identification. Likewise, if you consider that your right to personal data protection has been violated, you may file a complaint with the Andalusian Data Protection and Transparency Council www.ctpdandalucia.es