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Syllabus 2020-21 - 10312012 - Inorganic Chemistry Lab 2 (Laboratorio de química inorgánica II)
- Level 1: Tutorial support sessions, materials and exams in this language
- Level 2: Tutorial support sessions, materials, exams and seminars in this language
- Level 3: Tutorial support sessions, materials, exams, seminars and regular lectures in this language
DEGREE: | Grado en Químicas |
FACULTY: | FACULTY OF EXPERIMENTAL SCIENCES |
ACADEMIC YEAR: | 2020-21 |
COURSE: | Inorganic Chemistry Lab 2 |
NAME: Inorganic Chemistry Lab 2 | |||||
CODE: 10312012 | ACADEMIC YEAR: 2020-21 | ||||
LANGUAGE: English | LEVEL: 1 | ||||
ECTS CREDITS: 6.0 | YEAR: 3 | SEMESTER: PC |
NAME: ILLÁN CABEZA, NURIA ANTONIA | ||
DEPARTMENT: U128 - QUÍMICA INORGÁNICA Y ORGÁNICA | ||
FIELD OF STUDY: 760 - QUÍMICA INORGÁNICA | ||
OFFICE NO.: B3 - 449 | E-MAIL: naillan@ujaen.es | P: 953212949 |
WEBSITE: - | ||
ORCID: https://orcid.org/0000-0002-1646-8383 | ||
LANGUAGE: English | LEVEL: 1 |
0.- Description of the course. Aim and scope, contents and methodology. Bibliography. Assessment.
1.- Advanced synthesis of inorganic compounds
- Co(III) complexes
[Co(NH
3)
6]Cl
3
[CoCl(NH
3)
5]Cl
2
[Co(CO
3)(NH
3)
4]NO
3
[Co(NO
2)(NH
3)
5Cl
2
[Co(ONO)(NH
3)
5]Cl
2
- Ni(II) complexes
[Ni(NH
3)
6]Cl
2
K
2[Ni(CN)
4]·H
2O
[Ni(en)
3]Cl
2
- Otther compounds
K
3[Fe(C
2O
4)
3]·3H
2O
Thermochromic solids Cu
2[HgI
4] y Ag
2[HgI
4]
Adduct BH
3:NH
2C(CH
3)
3
2.- Instrumentation
- Conductivity measurements on coordination compounds
- UV-VIS-NIR spectroscopy
- Infrared spectroscopy
- Magnetic measurements
- Thermal analysis
A2- Practical sessions in labs to "small group" (58h )
The sessions (four hours each) will be devoted to the advanced synthesis of inorganic compounds and the application of instrumental techniques for the characterization of inorganic compounds.
· A3- Collective tutorials (2 h)
Students with special educational needs should contact the Student Attention Service (Servicio de Atención y Ayudas al Estudiante) in order to receive the appropriate academic support
ASSESSED COMPETENCES:
S1 Attendance and exercises (10%): B8, P5
S2 Exam (50%): P5, CE3, CE16
S4 Daily work and lab notebook (40%): P1, P3, P5, B8, B10,
CE3
WARNING :
1.- To pass the course, attendance at lab sessions is mandatory.
2.- Individual parts of the assessment must be passed separately.
3.- In the exam, basic mistakes -such as formulation, stoichiometry, periodic table, electronic configurations, etc.- will lead to the total cancellation of the question.
4.- In order to accomplish the provisions of the rules of assessment and academic regime (art. 18.4), the extraordinary exam will comprise the same three parts assessed in the ordinary call.
- The synthesis and characterization of inorganic compounds. Edition: -. Author: Jolly, William L.. Publisher: Prospect Heights, Ill. : Waveland Press, 1991, c1970. (Library)
- Experimental methods in inorganic chemistry. Edition: -. Author: Tanaka, John. Publisher: Upper Saddler River: Prentice Hall, cop. 1999 (Library)
- Inorganic experiments. Edition: 3rd rev. ed.. Author: -. Publisher: Weinheim : Wiley-VCH, 2010. (Library)
- Synthesis and technique in inorganic chemistry: a laboratory manual. Edition: 3rd ed. Author: Girolami, Gregory S.. Publisher: Sausalito: University Science Books, cop. 1999 (Library)
- Spectacular chemical experiments. Edition: -. Author: Roesky, H. W.. Publisher: Weinheim : Wiley-VCH, cop. 2007. (Library)
- Microscale general chemistry laboratory: with selected macroscale experiments. Edition: -. Author: Szafran, Zvi. Publisher: New York : Wiley, cop. 2003. (Library)
- Hazards in the chemical laboratory. Edition: 5th ed.. Author: -. Publisher: Cambridge : Royal Society of Chemistry, 1992. (Library)
- Structural methods in inorganic chemistry. Edition: 2nd ed. Author: Ebsworth, E. A. V. Publisher: Boca Raton, Fla. : CRC Press, c1991 (Library)
Formative activities
· Practical lessons in laboratory to a "small group" (58 h)
Format: presential (related to socialsanitary conditions in that moment)
· Collective tutorials (2 h), face-to-face format (related to socialsanitary conditions in that moment)
· Individual Tutorials
It could be done: (a) with appointment by Hangouts Meet (hour, day and link to videoconference will be sent by email), (b) by email and (c) forum from ILIAS platform. If sanitary conditions are favorable, face-to-face tutorials could be considered.
Changes in organization will be advised in anticipation.
ASSESSMENT METHODOLOGY
· Ordinary and extraordinary Call
- Attendance and exercises (10%)
- Exam (50%) (presential)
- Daily work and lab notebook (40%)
WARNING :
1.- To pass the course, attendance at lab sessions is mandatory.
2.- Individual parts of the assessment must be passed separately.
3.- In the exam, basic mistakes -such as formulation, stoichiometry, periodic table, electronic configurations, etc.- will lead to the total cancellation of the question.
4.- In order to accomplish the provisions of the rules of assessment and academic regime (art. 18.4), the extraordinary exam will comprise the same three parts assessed in the ordinary call.
Resources
Computer with microphone, webcam, Internet
connection (or smartphone). Telematic sessions will use
technical media supplied by University of Jaén
(ILIAS platform, Google Suite tools).
Electronic
books.
Formative activities
· Practical lessons in laboratory to a "small group" (58 h)
Format: online
· Collective tutorials (2 h), online format
· Individual Tutorials
It could be done: (a) with appointment by Hangouts Meet (hour, day and link to videoconference will be sent by email), (b) by email and (c) forum from ILIAS platform.
ASSESSMENT METHODOLOGY
· Ordinary and extraordinary Call
- Attendance and exercises (10%)
- Written/oral exam (online) (50%)
- Daily work and lab notebook (40%)
WARNING :
1.- To pass the course, attendance at lab sessions is mandatory.
2.- Individual parts of the assessment must be passed separately.
3.- In the exam, basic mistakes -such as formulation, stoichiometry, periodic table, electronic configurations, etc.- will lead to the total cancellation of the question.
4.- In order to accomplish the provisions of the rules of assessment and academic regime (art. 18.4), the extraordinary exam will comprise the same three parts assessed in the ordinary call.
Resources
Computer with microphone, webcam,
Internet connection
(or smartphone). Telematic sessions will use technical
media supplied by University of Jaén (ILIAS
platform, Google Suite tools).
Electronic books.
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