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Syllabus 2020-21 - 10312012 - Inorganic Chemistry Lab 2 (Laboratorio de química inorgánica II)

Caption
  • Level 1: Tutorial support sessions, materials and exams in this language
  • Level 2: Tutorial support sessions, materials, exams and seminars in this language
  • Level 3: Tutorial support sessions, materials, exams, seminars and regular lectures in this language
DEGREE: Grado en Químicas
FACULTY: FACULTY OF EXPERIMENTAL SCIENCES
ACADEMIC YEAR: 2020-21
COURSE: Inorganic Chemistry Lab 2
SYLLABUS
1. COURSE BASIC INFORMATION
NAME: Inorganic Chemistry Lab 2
CODE: 10312012 ACADEMIC YEAR: 2020-21
LANGUAGE: English LEVEL: 1
ECTS CREDITS: 6.0 YEAR: 3 SEMESTER: PC
2. LECTURER BASIC INFORMATION
NAME: ILLÁN CABEZA, NURIA ANTONIA
DEPARTMENT: U128 - QUÍMICA INORGÁNICA Y ORGÁNICA
FIELD OF STUDY: 760 - QUÍMICA INORGÁNICA
OFFICE NO.: B3 - 449 E-MAIL: naillan@ujaen.es P: 953212949
WEBSITE: -
ORCID: https://orcid.org/0000-0002-1646-8383
LANGUAGE: English LEVEL: 1
3. CONTENT DESCRIPTION

0.- Description of the course. Aim and scope, contents and methodology. Bibliography. Assessment.

1.- Advanced synthesis of inorganic compounds

- Co(III) complexes

[Co(NH 3) 6]Cl 3
[CoCl(NH 3) 5]Cl 2
[Co(CO 3)(NH 3) 4]NO 3
[Co(NO 2)(NH 3) 5Cl 2
[Co(ONO)(NH 3) 5]Cl 2

- Ni(II) complexes 
[Ni(NH 3) 6]Cl 2
K 2[Ni(CN) 4]·H 2O
[Ni(en) 3]Cl 2
- Otther compounds 
K 3[Fe(C 2O 4) 3]·3H 2O
Thermochromic solids Cu 2[HgI 4] y Ag 2[HgI 4]
Adduct BH 3:NH 2C(CH 3) 3

2.- Instrumentation

- Conductivity measurements on coordination compounds
- UV-VIS-NIR spectroscopy
- Infrared spectroscopy
- Magnetic measurements
- Thermal analysis

4. COURSE DESCRIPTION AND TEACHING METHODOLOGY

A2- Practical sessions in labs to "small group" (58h )

The sessions (four hours each) will be devoted to the advanced synthesis of inorganic compounds and the application of instrumental techniques for the characterization of inorganic compounds.

· A3- Collective tutorials (2 h)

Students with special educational needs should contact the Student Attention Service (Servicio de Atención y Ayudas al Estudiante) in order to receive the appropriate academic support

5. ASSESSMENT METHODOLOGY

ASSESSED COMPETENCES:

S1 Attendance and exercises (10%): B8, P5
S2 Exam (50%): P5, CE3, CE16
S4 Daily work and lab notebook (40%): P1, P3, P5, B8, B10, CE3

WARNING :

1.- To pass the course, attendance at lab sessions is mandatory.

2.-  Individual parts of the assessment must be passed separately.

3.- In the exam, basic mistakes -such as formulation, stoichiometry, periodic table, electronic configurations, etc.- will lead to the total cancellation of the question.

4.- In order to accomplish the provisions of the rules of assessment and academic regime (art. 18.4), the extraordinary exam will comprise the same three parts assessed in the ordinary call.

6. BOOKLIST
MAIN BOOKLIST:
  • The synthesis and characterization of inorganic compounds. Edition: -. Author: Jolly, William L.. Publisher: Prospect Heights, Ill. : Waveland Press, 1991, c1970.  (Library)
  • Experimental methods in inorganic chemistry. Edition: -. Author: Tanaka, John. Publisher: Upper Saddler River: Prentice Hall, cop. 1999  (Library)
  • Inorganic experiments. Edition: 3rd rev. ed.. Author: -. Publisher: Weinheim : Wiley-VCH, 2010.  (Library)
  • Synthesis and technique in inorganic chemistry: a laboratory manual. Edition: 3rd ed. Author: Girolami, Gregory S.. Publisher: Sausalito: University Science Books, cop. 1999  (Library)
ADDITIONAL BOOKLIST:
  • Spectacular chemical experiments. Edition: -. Author: Roesky, H. W.. Publisher: Weinheim : Wiley-VCH, cop. 2007.  (Library)
  • Microscale general chemistry laboratory: with selected macroscale experiments. Edition: -. Author: Szafran, Zvi. Publisher: New York : Wiley, cop. 2003.  (Library)
  • Hazards in the chemical laboratory. Edition: 5th ed.. Author: -. Publisher: Cambridge : Royal Society of Chemistry, 1992.  (Library)
  • Structural methods in inorganic chemistry. Edition: 2nd ed. Author: Ebsworth, E. A. V. Publisher: Boca Raton, Fla. : CRC Press, c1991  (Library)
8. VIRTUAL / CLASSROOM TEACHING SCENARIO

Formative activities

· Practical lessons in laboratory to a "small group" (58 h)

Format: presential (related to socialsanitary conditions in that moment)

· Collective tutorials (2 h), face-to-face format (related to socialsanitary conditions in that moment)

· Individual Tutorials

It could be done:  (a) with appointment by Hangouts Meet (hour, day and link to videoconference will be sent by email), (b) by email and (c) forum from ILIAS platform. If sanitary conditions are favorable, face-to-face tutorials could be considered.

 Changes in organization will be advised in anticipation.

ASSESSMENT METHODOLOGY

· Ordinary and extraordinary Call

- Attendance and exercises (10%)

- Exam (50%) (presential)

- Daily work and lab notebook (40%)

WARNING :

1.- To pass the course, attendance at lab sessions is mandatory.

2.-  Individual parts of the assessment must be passed separately.

3.- In the exam, basic mistakes -such as formulation, stoichiometry, periodic table, electronic configurations, etc.- will lead to the total cancellation of the question.

4.- In order to accomplish the provisions of the rules of assessment and academic regime (art. 18.4), the extraordinary exam will comprise the same three parts assessed in the ordinary call.

Resources  
  Computer with microphone, webcam, Internet connection (or smartphone). Telematic sessions will use technical media supplied  by University of Jaén (ILIAS platform, Google Suite tools).  
Electronic books.

9. VIRTUAL TEACHING SCENARIO

Formative activities

· Practical lessons in laboratory to a "small group" (58 h)

Format: online

· Collective tutorials (2 h), online format

· Individual Tutorials

It could be done:  (a) with appointment by Hangouts Meet (hour, day and link to videoconference will be sent by email), (b) by email and (c) forum from ILIAS platform.

ASSESSMENT METHODOLOGY

· Ordinary and extraordinary Call

- Attendance and exercises (10%)

- Written/oral exam (online) (50%) 

- Daily work and lab notebook (40%)

WARNING :

1.- To pass the course, attendance at lab sessions is mandatory.

2.-  Individual parts of the assessment must be passed separately.

3.- In the exam, basic mistakes -such as formulation, stoichiometry, periodic table, electronic configurations, etc.- will lead to the total cancellation of the question.

4.- In order to accomplish the provisions of the rules of assessment and academic regime (art. 18.4), the extraordinary exam will comprise the same three parts assessed in the ordinary call.

Resources
 
Computer with microphone, webcam, Internet connection
(or smartphone). Telematic sessions will use technical media supplied  by University of Jaén (ILIAS platform, Google Suite tools). 
Electronic books.

DATA PROTECTION CLAUSE (on line exams)

Institution in charge of data processing: Universidad de Jaén, Campus Las Lagunillas, s/n, 23071 Jaén

Data Protection Delegate: dpo@ujaen.es

Purpose: In accordance with the Universities Law and other national and regional regulations in force, carrying out exams and assessment tests corresponding to the courses students are registered in. In order to avoid frauds while sitting the exam, the exam will be answered using a videoconference system, being able the academic staff of the University of Jaén to compare and contrast the image of the person who is answering the exam with the student's photographic files. Likewise, in order to provide the exam with evidential content for revisions or claims, in accordance with current regulation frameworks, the exam will be recorded and stored.

Legitimacy: compliance with legal obligations (Universities Law) and other national and regional regulations currently in force.

Addressees: service providers who are the owners of the platforms where the exams are carried out and with whom the University of Jaén has signed the corresponding data access contracts.

Storage periods: those established in current in force regulations. In the specific case of exam videoconference recordings, not before the examination records and transcripts are closed or the exam can still be reviewed or challenged.

Rights: you can exercise your right of access, amendment, cancellation, opposition, suppression, limitation and portability by sending a letter to the postal or electronic address indicated above. In the event that you consider that your rights have been violated, you may submit a complaint to the Andalusian Council for Transparency and Data Protection www.ctpdandalucia.es

CLASS RECORDING CLAUSE PERSONAL DATA PROTECTION

Person in charge: Universidad de Jaén, Paraje Las Lagunillas, s/n; Tel.953 212121; www.ujaen.es

Data protection delegate (DPO): TELEFÓNICA, S.A.U. ; Email: dpo@ujaen.es

Procedure aim: To manage proper recordings of teaching sessions with the aim of facilitating learning process under a multimodal and/or online teaching

Period for record storage: Images will be kept during legal term according to regulations in force

Legitimacy: Data will be managed according to legal regulations (Organic Law 6/2001, December 21, on Universities) and given consent provided by selecting corresponding box in legal admission documents

Data recipients (transfers or assignments): Any person allowed to get access to every teaching modality

Rights: You may exercise your rights of access, rectification, cancellation, portability, limitation of processing, deletion or, where appropriate, opposition. To exercise these rights, you must submit a written request to the Information, Registration and Electronic Administration Service of the University of Jaen at the address above, or by e-mail to the address above. You must specify which of these rights you are requesting to be satisfied and, at the same time, you must attach a photocopy of your ID card or equivalent identification document. In case you act through a representative, legal or voluntary, you must also provide a document that proves this representation and identification. Likewise, if you consider that your right to personal data protection has been violated, you may file a complaint with the Andalusian Data Protection and Transparency Council www.ctpdandalucia.es