Universidad de Jaén

Menú local

Syllabus 2018-19 - 10312012 - Inorganic Chemistry Lab 2 (Laboratorio de química inorgánica II)

Caption
  • Level 1: Tutorial support sessions, materials and exams in this language
  • Level 2: Tutorial support sessions, materials, exams and seminars in this language
  • Level 3: Tutorial support sessions, materials, exams, seminars and regular lectures in this language
DEGREE: Grado en Químicas
FACULTY: FACULTY OF EXPERIMENTAL SCIENCES

ACADEMIC YEAR: 2018-19
SYLLABUS
1. COURSE BASIC INFORMATION
NAME: Inorganic Chemistry Lab 2
CODE: 10312012 ACADEMIC YEAR: 2018-19
LANGUAGE: English LEVEL: 1
ECTS CREDITS: 6.0 YEAR: 3 SEMESTER: PC
 
2. LECTURER BASIC INFORMATION
NAME: MORENO CARRETERO, MIGUEL NICOLÁS
DEPARTMENT: U128 - QUÍMICA INORGÁNICA Y ORGÁNICA
FIELD OF STUDY: 760 - QUÍMICA INORGÁNICA
OFFICE NO.: B3 - B3-445 E-MAIL: mmoreno@ujaen.es P: 953212738
WEBSITE: http://www4.ujaen.es/~mmoreno/index.htm
LANGUAGE: English LEVEL: 1
 
3. CONTENT DESCRIPTION

0.- Description of the course. Aim and scope, contents and methodology. Bibliography. Assessment.

1.- Advanced synthesis of inorganic compounds

- Co(III) complexes

[Co(NH 3) 6]Cl 3
[CoCl(NH 3) 5]Cl 2
[Co(CO 3)(NH 3) 4]NO 3
[Co(NO 2)(NH 3) 5Cl 2
[Co(ONO)(NH 3) 5]Cl 2

- Ni(II) complexes 
[Ni(NH 3) 6]Cl 2
K 2[Ni(CN) 4]·H 2O
[Ni(en) 3]Cl 2
- Otther compounds 
K 3[Fe(C 2O 4) 3]·3H 2O
Zeolite A
Thermochromic solids Cu 2[HgI 4] y Ag 2[HgI 4]
Adduct BH 3:NH 2C(CH 3) 3

2.- Instrumentation

- Conductivity measurements on coordination compounds
- UV-VIS-NIR spectroscopy
- Infrared spectroscopy
- Magnetic measurements
- Thermal analysis

4. COURSE DESCRIPTION AND TEACHING METHODOLOGY

The nine first sessions (four hours each) will be devoted to the synthesis and characterization of compounds.The remaining sessions will be used in seminars on Instrumental Techniques. During the last session, the exam will be done.

Students with special educational needs should contact the Student Attention Service (Servicio de Atención y Ayudas al Estudiante) in order to receive the appropriate academic support

5. ASSESSMENT METHODOLOGY

ASSESSED COMPETENCES:

S1 Attendance and exercises (10%): B8, P5
S2 Exam (30%): P5, CE3, CE16
S4 Daily work and lab notebook (60%): P1, P3, P5, B8, B10, CE3

WARNING :

1.- To pass the course, attendance at lab sessions is mandatory.

2.-  Individual parts of the assessment must be passed separately.

3.- In the exam, basic mistakes -such as formulation, stoichiometry, periodic table, electronic configurations, etc.- will lead to the total cancellation of the question.

4.- In order to accomplish the provisions of the rules of assessment and academic regime (art. 18.4), the extraordinary exam will comprise the same three parts assessed in the ordinary call.

6. BOOKLIST
MAIN BOOKLIST:
  • The synthesis and characterization of inorganic compounds. Edition: -. Author: Jolly, William L.. Publisher: Prospect Heights, Ill. : Waveland Press, 1991, c1970.  (Library)
  • Experimental methods in inorganic chemistry. Edition: -. Author: Tanaka, John. Publisher: Upper Saddler River: Prentice Hall, cop. 1999  (Library)
  • Inorganic experiments. Edition: 3rd rev. ed.. Author: -. Publisher: Weinheim : Wiley-VCH, 2010.  (Library)
  • Synthesis and technique in inorganic chemistry: a laboratory manual. Edition: 3rd ed. Author: Girolami, Gregory S.. Publisher: Sausalito: University Science Books, cop. 1999  (Library)
ADDITIONAL BOOKLIST:
  • Spectacular chemical experiments. Edition: -. Author: Roesky, H. W.. Publisher: Weinheim : Wiley-VCH, cop. 2007.  (Library)
  • Microscale general chemistry laboratory: with selected macroscale experiments. Edition: -. Author: Szafran, Zvi. Publisher: New York : Wiley, cop. 2003.  (Library)
  • Hazards in the chemical laboratory. Edition: 5th ed.. Author: -. Publisher: Cambridge : Royal Society of Chemistry, 1992.  (Library)
  • Structural methods in inorganic chemistry. Edition: 2nd ed. Author: Ebsworth, E. A. V. Publisher: Boca Raton, Fla. : CRC Press, c1991  (Library)