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Syllabus 2015-16 - 10312004 - Analytical Chemistry Lab (Laboratorio de química analítica)

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  • Level 1: Tutorial support sessions, materials and exams in this language
  • Level 2: Tutorial support sessions, materials, exams and seminars in this language
  • Level 3: Tutorial support sessions, materials, exams, seminars and regular lectures in this language
DEGREE: Grado en Químicas
FACULTY: FACULTY OF EXPERIMENTAL SCIENCES
ACADEMIC YEAR: 2015-16
COURSE: Analytical Chemistry Lab
SYLLABUS
1. COURSE BASIC INFORMATION
NAME: Analytical Chemistry Lab
CODE: 10312004 ACADEMIC YEAR: 2015-16
LANGUAGE: English LEVEL: 1
ECTS CREDITS: 6.0 YEAR: 3 SEMESTER: SC
2. LECTURER BASIC INFORMATION
NAME: MOLINA DÍAZ, ANTONIO
DEPARTMENT: U127 - QUIMÍCA FÍSICA Y ANALÍTICA
FIELD OF STUDY: 750 - QUÍMICA ANALÍTICA
OFFICE NO.: B3 - 138 E-MAIL: amolina@ujaen.es P: 953212147
WEBSITE: -
ORCID: https://orcid.org/0000-0003-2380-192X
LANGUAGE: English LEVEL: 1
3. CONTENT DESCRIPTION

This is an Analytical Chemistry laboratory course,  with a series of practical works involving those instrumental analytical techniques which are fundamental to Chemistry Grade students.

 

Contents:

 

The students will perform the following practices:

1.        Spectrophotometric determination of phosphorus in soil samples

2.      Determination of an iron and aluminum mixture by using selective extraction with oxine .

3.      Spectrophotometric determination of polyphenols in foods.

4.      Determination of sodium and potassium in wine, milk and serum by flame atomic emission.

5.      Determination of chromium in steels by flame atomic absorption spectroscopy: validation of an analytical method.

6.      Potentiometric determination of fluoride in drinking water, mouthwash and toothpaste by using ion selective electrodes

7.      Conductimetric determinación of  vinegar acidity

8.      Determination of phenols in water by means of liquid chromatography and solid phase extraction.

9.  Determination of a pharmaceutical mixture by HPLC.

10.  Determination of organochlorine pesticides by means of Gas Chromatography.

11.    Characterizing physical parameters of a flow injection system. Determination of t hiocyanate.

12.  Determination of metals in waters by ICP-MS.

 

4. COURSE DESCRIPTION AND TEACHING METHODOLOGY

Laboratory work and additional activities 

Students with special educational needs should contact the Student Attention Service (Servicio de Atención y Ayudas al Estudiante) in order to receive the appropriate academic support

5. ASSESSMENT METHODOLOGY

Exam paper combined with the evaluation of a proposed activity

6. BOOKLIST
MAIN BOOKLIST:
  • Principles of instrumental analysis. Edition: 6th ed.. Author: Skoog, Douglas A.. Publisher: Belmont, CA: Thomson, cop. 2007  (Library)
  • Automatic methods of analysis. Edition: -. Author: Valcárcel Cases, M.. Publisher: Amsterdam [etc.]: Elsevier, 1988  (Library)
ADDITIONAL BOOKLIST:
  • Analytical instrumentation handbook. Edition: 2nd ed. rev. and exp.. Author: -. Publisher: New York : Marcel Dekker , 1997.  (Library)